Optimisation of ultrasound-assisted extraction of rosehip (Rosa canina L.) with response surface methodology


Ilbay Z., ŞAHİN SEVGİLİ S., KIRBAŞLAR Ş. İ.

Journal of the Science of Food and Agriculture, vol.93, no.11, pp.2804-2809, 2013 (SCI-Expanded) identifier identifier

  • Publication Type: Article / Article
  • Volume: 93 Issue: 11
  • Publication Date: 2013
  • Doi Number: 10.1002/jsfa.6104
  • Journal Name: Journal of the Science of Food and Agriculture
  • Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Page Numbers: pp.2804-2809
  • Keywords: Optimisation, Polyphenols, Rosa canina L, RSM, Ultrasound-assisted extraction
  • Uşak University Affiliated: No

Abstract

Background: Ultrasound-assisted extraction of polyphenols from rosehip (Rosa canina L.) was investigated. The aim of the study was to examine the extraction parameters such as extraction time (30-90min), temperature (30-50°C) and solvent concentration (40-100% ethanol, v/v), and to obtain the best possible combinations of these parameters by using response surface methodology. Results: The experiments were performed according to the face-centred central design. Total phenolic content was expressed in gallic acid equivalent (GAE) per gram of dried matter (DM). The second-order polynomial model gave a satisfactory description of the experimental data. 47.23mg GAE g-1 DM was predicted at the optimum operating conditions (40% EtOH composition, 50°C of temperature, and 81.23min of extraction time). Conclusion: All of the parameters (ethanol concentration, extraction time and extraction temperature) used in this research have the significant effect on the extraction efficiency of total phenolic content in rosehip extracts (P<0.05). The solvent concentration was proved to be the most significant effective on the yields obtained by ultrasound-assisted extraction. © 2013 Society of Chemical Industry.