SYNTHESIS, CHARACTERIZATION AND THERMAL PROPERTIES OF NEW OXOETHYL ACRYLATE CONTAINING POLYMER

ÇANKAYA N.

Sigma Journal of Engineering and Natural Sciences, vol.38, no.1, pp.281-288, 2020 (ESCI) identifier

  • Publication Type: Article / Article
  • Volume: 38 Issue: 1
  • Publication Date: 2020
  • Journal Name: Sigma Journal of Engineering and Natural Sciences
  • Journal Indexes: Emerging Sources Citation Index (ESCI), Scopus, Academic Search Premier, Directory of Open Access Journals
  • Page Numbers: pp.281-288
  • Keywords: 2-(bis(cyanomethyl)amino)-2-oxoethyl acrylate (CMA2OEA), homopolymer, monomer, poly(CMA2OEA), synthesis and characterization, thermal stability
  • Uşak University Affiliated: Yes

Abstract

In this study, 2-(bis(cyanomethyl)amino)-2-oxoethyl acrylate (CMA2OEA) monomer, which does not exist in the literature, was synthesized and characterized. Elemental analysis technique, along with classical spectroscopic methods such as FTIR, 1H and 13C NMR, is used in the characterization of the monomer. Further, homopolymer of the CMA2OEA monomer [poly(CMA2OEA)] is synthesized by free radical chain polymerization reaction. Homopolymer synthesized is also characterized by spectroscopic techniques and thermal characterization is investigated by TGA/DTA/DTG thermal analysis methods.