SYNTHESIS, CHARACTERIZATION AND THERMAL PROPERTIES OF NEW OXOETHYL ACRYLATE CONTAINING POLYMER

ÇANKAYA N.

Sigma Journal of Engineering and Natural Sciences, cilt.38, sa.1, ss.281-288, 2020 (ESCI) identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 38 Sayı: 1
  • Basım Tarihi: 2020
  • Dergi Adı: Sigma Journal of Engineering and Natural Sciences
  • Derginin Tarandığı İndeksler: Emerging Sources Citation Index (ESCI), Scopus, Academic Search Premier, Directory of Open Access Journals
  • Sayfa Sayıları: ss.281-288
  • Anahtar Kelimeler: 2-(bis(cyanomethyl)amino)-2-oxoethyl acrylate (CMA2OEA), homopolymer, monomer, poly(CMA2OEA), synthesis and characterization, thermal stability
  • Uşak Üniversitesi Adresli: Evet

Özet

In this study, 2-(bis(cyanomethyl)amino)-2-oxoethyl acrylate (CMA2OEA) monomer, which does not exist in the literature, was synthesized and characterized. Elemental analysis technique, along with classical spectroscopic methods such as FTIR, 1H and 13C NMR, is used in the characterization of the monomer. Further, homopolymer of the CMA2OEA monomer [poly(CMA2OEA)] is synthesized by free radical chain polymerization reaction. Homopolymer synthesized is also characterized by spectroscopic techniques and thermal characterization is investigated by TGA/DTA/DTG thermal analysis methods.